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Waxberry-like magnetic porous carbon composites prepared from a nickel-organic framework for solid-phase extraction of fluoroquinolones

A unique waxberry-like magnetic hierarchical porous carbon hybrid was synthesized from a nickel based metal–organic framework (Ni-MOF) which, on calcination, produces hierarchical Ni/NiO nanocrystals covered with graphitic carbon (GrC). The material was applied to magnetic solid phase extraction (MS... Full description

Journal Title: Mikrochimica acta (1966) 2017-08-08, Vol.184 (10), p.4107-4115
Main Author: Wang, Qiong
Other Authors: Wang, Yang , Zhang, Zhenzhen , Tong, Yao , Zhang, Lei
Format: Electronic Article Electronic Article
Language: English
Subjects:
Publisher: Vienna: Springer Vienna
ID: ISSN: 0026-3672
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title: Waxberry-like magnetic porous carbon composites prepared from a nickel-organic framework for solid-phase extraction of fluoroquinolones
format: Article
creator:
  • Wang, Qiong
  • Wang, Yang
  • Zhang, Zhenzhen
  • Tong, Yao
  • Zhang, Lei
subjects:
  • Adsorption
  • Analytical Chemistry
  • Boron nitride
  • Carbon
  • Characterization and Evaluation of Materials
  • Chemistry
  • Chemistry and Materials Science
  • Extraction
  • Fish
  • Magnetism
  • Microengineering
  • Nanochemistry
  • Nanotechnology
  • Nickel
  • Original Paper
  • Protozoa
  • Reusable components
  • Signal to noise ratio
ispartof: Mikrochimica acta (1966), 2017-08-08, Vol.184 (10), p.4107-4115
description: A unique waxberry-like magnetic hierarchical porous carbon hybrid was synthesized from a nickel based metal–organic framework (Ni-MOF) which, on calcination, produces hierarchical Ni/NiO nanocrystals covered with graphitic carbon (GrC). The material was applied to magnetic solid phase extraction (MSPE) of trace levels of four fluoroquinolones (FQs) from environmental water samples. It is shown to exhibit superior extraction capability for four FQs, because the novel 3D morphology provides an enhanced surface area along with transport channels, while Ni and graphitic carbon as potential adsorption sites are ideal components. The material with inherent magnetism is reusable and displays superb recycling stability for the adsorption and desorption (by using alkaline methanol) of FQs after 6 cycles. The FQs were quantified by HPLC with UV detection, and the limits of detection (at an S/N ratio of 3) range between 7.9 and 57 ng·L −1 . Recoveries from spiked environmental water samples are between 88.8 and 103.7%. Graphical Abstract A magnetic hierarchical porous carbon hybrid was prepared from a nickel-organic framework and applied to solid phase extraction of trace levels fluoroquinolones from environmental water samples.
language: eng
source:
identifier: ISSN: 0026-3672
fulltext: no_fulltext
issn:
  • 0026-3672
  • 1436-5073
url: Link


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titleWaxberry-like magnetic porous carbon composites prepared from a nickel-organic framework for solid-phase extraction of fluoroquinolones
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descriptionA unique waxberry-like magnetic hierarchical porous carbon hybrid was synthesized from a nickel based metal–organic framework (Ni-MOF) which, on calcination, produces hierarchical Ni/NiO nanocrystals covered with graphitic carbon (GrC). The material was applied to magnetic solid phase extraction (MSPE) of trace levels of four fluoroquinolones (FQs) from environmental water samples. It is shown to exhibit superior extraction capability for four FQs, because the novel 3D morphology provides an enhanced surface area along with transport channels, while Ni and graphitic carbon as potential adsorption sites are ideal components. The material with inherent magnetism is reusable and displays superb recycling stability for the adsorption and desorption (by using alkaline methanol) of FQs after 6 cycles. The FQs were quantified by HPLC with UV detection, and the limits of detection (at an S/N ratio of 3) range between 7.9 and 57 ng·L −1 . Recoveries from spiked environmental water samples are between 88.8 and 103.7%. Graphical Abstract A magnetic hierarchical porous carbon hybrid was prepared from a nickel-organic framework and applied to solid phase extraction of trace levels fluoroquinolones from environmental water samples.
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subjectAdsorption ; Analytical Chemistry ; Boron nitride ; Carbon ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Extraction ; Fish ; Magnetism ; Microengineering ; Nanochemistry ; Nanotechnology ; Nickel ; Original Paper ; Protozoa ; Reusable components ; Signal to noise ratio
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abstractA unique waxberry-like magnetic hierarchical porous carbon hybrid was synthesized from a nickel based metal–organic framework (Ni-MOF) which, on calcination, produces hierarchical Ni/NiO nanocrystals covered with graphitic carbon (GrC). The material was applied to magnetic solid phase extraction (MSPE) of trace levels of four fluoroquinolones (FQs) from environmental water samples. It is shown to exhibit superior extraction capability for four FQs, because the novel 3D morphology provides an enhanced surface area along with transport channels, while Ni and graphitic carbon as potential adsorption sites are ideal components. The material with inherent magnetism is reusable and displays superb recycling stability for the adsorption and desorption (by using alkaline methanol) of FQs after 6 cycles. The FQs were quantified by HPLC with UV detection, and the limits of detection (at an S/N ratio of 3) range between 7.9 and 57 ng·L −1 . Recoveries from spiked environmental water samples are between 88.8 and 103.7%. Graphical Abstract A magnetic hierarchical porous carbon hybrid was prepared from a nickel-organic framework and applied to solid phase extraction of trace levels fluoroquinolones from environmental water samples.
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doi10.1007/s00604-017-2438-2