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Study on the Photocatalytic Degradation of Methyl Orange in Water Using Ag/ZnO as Catalyst by Liquid Chromatography Electrospray Ionization Ion-Trap Mass Spectrometry

A nanocrystal catalyst Ag/ZnO was successfully synthesized using a simple solvothermal method in this study. This catalyst was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results showed that this catalyst was composed of metallic Ag and ZnO. The photodegr... Full description

Journal Title: Journal of the American Society for Mass Spectrometry 2008, Vol.19 (7), p.997-1003
Main Author: Chen, Tianwen
Other Authors: Zheng, Yuanhui , Lin, Jin-Ming , Chen, Guonan
Format: Electronic Article Electronic Article
Language: English
Subjects:
Publisher: New York: Elsevier Inc
ID: ISSN: 1044-0305
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recordid: cdi_proquest_miscellaneous_69289941
title: Study on the Photocatalytic Degradation of Methyl Orange in Water Using Ag/ZnO as Catalyst by Liquid Chromatography Electrospray Ionization Ion-Trap Mass Spectrometry
format: Article
creator:
  • Chen, Tianwen
  • Zheng, Yuanhui
  • Lin, Jin-Ming
  • Chen, Guonan
subjects:
  • Analysis
  • Analytical Chemistry
  • Applied sciences
  • Article
  • Azo compounds
  • Bioinformatics
  • Biotechnology
  • Chemistry
  • Chemistry and Materials Science
  • Chromatographic methods and physical methods associated with chromatography
  • Electron microscopy
  • Exact sciences and technology
  • Fertilizers
  • Food
  • General and physical chemistry
  • General purification processes
  • Liquid chromatography
  • Mass spectrometry
  • Organic Chemistry
  • Other chromatographic methods
  • Photochemistry
  • Physical chemistry of induced reactions (with radiations, particles and ultrasonics)
  • Pollution
  • Proteomics
  • Safety and security measures
  • Universities and colleges
  • Wastewaters
  • Water treatment and pollution
  • Zinc oxide
ispartof: Journal of the American Society for Mass Spectrometry, 2008, Vol.19 (7), p.997-1003
description: A nanocrystal catalyst Ag/ZnO was successfully synthesized using a simple solvothermal method in this study. This catalyst was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results showed that this catalyst was composed of metallic Ag and ZnO. The photodegradation of methyl orange (MO) was investigated in aqueous suspension containing Ag/ZnO catalyst under UV irradiation. Liquid chromatography coupled with electrospray ionization ion-trap mass spectrometry was applied to the analysis of the samples coming from the photocatalytic degradation of MO. The experimental results showed that there were four intermediates existing in the photocatalytic reaction. MO could be mineralized in the Ag/ZnO suspension after 60 min illumination.
language: eng
source:
identifier: ISSN: 1044-0305
fulltext: no_fulltext
issn:
  • 1044-0305
  • 1879-1123
url: Link


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titleStudy on the Photocatalytic Degradation of Methyl Orange in Water Using Ag/ZnO as Catalyst by Liquid Chromatography Electrospray Ionization Ion-Trap Mass Spectrometry
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descriptionA nanocrystal catalyst Ag/ZnO was successfully synthesized using a simple solvothermal method in this study. This catalyst was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results showed that this catalyst was composed of metallic Ag and ZnO. The photodegradation of methyl orange (MO) was investigated in aqueous suspension containing Ag/ZnO catalyst under UV irradiation. Liquid chromatography coupled with electrospray ionization ion-trap mass spectrometry was applied to the analysis of the samples coming from the photocatalytic degradation of MO. The experimental results showed that there were four intermediates existing in the photocatalytic reaction. MO could be mineralized in the Ag/ZnO suspension after 60 min illumination.
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subjectAnalysis ; Analytical Chemistry ; Applied sciences ; Article ; Azo compounds ; Bioinformatics ; Biotechnology ; Chemistry ; Chemistry and Materials Science ; Chromatographic methods and physical methods associated with chromatography ; Electron microscopy ; Exact sciences and technology ; Fertilizers ; Food ; General and physical chemistry ; General purification processes ; Liquid chromatography ; Mass spectrometry ; Organic Chemistry ; Other chromatographic methods ; Photochemistry ; Physical chemistry of induced reactions (with radiations, particles and ultrasonics) ; Pollution ; Proteomics ; Safety and security measures ; Universities and colleges ; Wastewaters ; Water treatment and pollution ; Zinc oxide
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descriptionA nanocrystal catalyst Ag/ZnO was successfully synthesized using a simple solvothermal method in this study. This catalyst was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results showed that this catalyst was composed of metallic Ag and ZnO. The photodegradation of methyl orange (MO) was investigated in aqueous suspension containing Ag/ZnO catalyst under UV irradiation. Liquid chromatography coupled with electrospray ionization ion-trap mass spectrometry was applied to the analysis of the samples coming from the photocatalytic degradation of MO. The experimental results showed that there were four intermediates existing in the photocatalytic reaction. MO could be mineralized in the Ag/ZnO suspension after 60 min illumination.
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abstractA nanocrystal catalyst Ag/ZnO was successfully synthesized using a simple solvothermal method in this study. This catalyst was characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The results showed that this catalyst was composed of metallic Ag and ZnO. The photodegradation of methyl orange (MO) was investigated in aqueous suspension containing Ag/ZnO catalyst under UV irradiation. Liquid chromatography coupled with electrospray ionization ion-trap mass spectrometry was applied to the analysis of the samples coming from the photocatalytic degradation of MO. The experimental results showed that there were four intermediates existing in the photocatalytic reaction. MO could be mineralized in the Ag/ZnO suspension after 60 min illumination.
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