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Synthesis and characterization of poly(1-vinyl-1,2,4-triazole) (PVTri)–barium hexaferrite nanocomposite

We present a method for the fabrication of PVTri–BaFe O nanocomposites by in-situ polymerization of PVTri in the presence of synthesized BaFe O nanoparticles. Nanoparticles, polymer and nanocomposite were analyzed by XRD, FTIR, TGA, TEM, NMR, GPC and conductivity techniques for structural and physic... Full description

Journal Title: Physica B: Physics of Condensed Matter 2011, Vol.406(11), pp.2298-2302
Main Author: Durmus, Z
Other Authors: Unal, B , Toprak, M.S , Aslan, A , Baykal, A
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: ISSN: 0921-4526 ; E-ISSN: 1873-2135 ; DOI: 10.1016/j.physb.2011.03.063
Link: https://www.sciencedirect.com/science/article/pii/S0921452611002948
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recordid: elsevier_sdoi_10_1016_j_physb_2011_03_063
title: Synthesis and characterization of poly(1-vinyl-1,2,4-triazole) (PVTri)–barium hexaferrite nanocomposite
format: Article
creator:
  • Durmus, Z
  • Unal, B
  • Toprak, M.S
  • Aslan, A
  • Baykal, A
subjects:
  • Nanocomposite
  • Hexaferrites
  • Electrical Properties
  • Poly(1-Vinyl-1,2,4-Triazole)
  • Engineering
  • Physics
ispartof: Physica B: Physics of Condensed Matter, 2011, Vol.406(11), pp.2298-2302
description: We present a method for the fabrication of PVTri–BaFe O nanocomposites by in-situ polymerization of PVTri in the presence of synthesized BaFe O nanoparticles. Nanoparticles, polymer and nanocomposite were analyzed by XRD, FTIR, TGA, TEM, NMR, GPC and conductivity techniques for structural and physicochemical characteristics. Crystallographic analysis revealed the phase as hexaferrite and X-ray line profile fitting yielded a crystallite size of 17±5 nm. Conjugation of PVTri to nanoparticle surface was assessed to be via carbonyl groups on the polymer. TG analysis revealed that 45 wt% of nanocomposite is inorganic phase (BaFe O ). It was found out that the ac conductivity of nanocomposite under a certain frequency increases with temperature.
language: eng
source:
identifier: ISSN: 0921-4526 ; E-ISSN: 1873-2135 ; DOI: 10.1016/j.physb.2011.03.063
fulltext: fulltext
issn:
  • 0921-4526
  • 09214526
  • 1873-2135
  • 18732135
url: Link


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titleSynthesis and characterization of poly(1-vinyl-1,2,4-triazole) (PVTri)–barium hexaferrite nanocomposite
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subjectNanocomposite ; Hexaferrites ; Electrical Properties ; Poly(1-Vinyl-1,2,4-Triazole) ; Engineering ; Physics
descriptionWe present a method for the fabrication of PVTri–BaFe O nanocomposites by in-situ polymerization of PVTri in the presence of synthesized BaFe O nanoparticles. Nanoparticles, polymer and nanocomposite were analyzed by XRD, FTIR, TGA, TEM, NMR, GPC and conductivity techniques for structural and physicochemical characteristics. Crystallographic analysis revealed the phase as hexaferrite and X-ray line profile fitting yielded a crystallite size of 17±5 nm. Conjugation of PVTri to nanoparticle surface was assessed to be via carbonyl groups on the polymer. TG analysis revealed that 45 wt% of nanocomposite is inorganic phase (BaFe O ). It was found out that the ac conductivity of nanocomposite under a certain frequency increases with temperature.
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