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Propylene oxide assisted one-pot, tandem synthesis of substituted-1,3,4-oxadiazole-2(3H)-ones in water

It has been developed for the synthesis of substituted-1,3,4-oxadiazole-2(3 )-one derivatives via a novel one-pot, tandem procedure assisted by propylene oxide. The 5-substitued-1,3,4-oxadiazole-2(3 )-ones and 3,5-disubstitued-1,3,4-oxadiazole-2(3 )-ones were, respectively, obtained from three-compo... Full description

Journal Title: Tetrahedron 23 September 2012, Vol.68(38), pp.7978-7983
Main Author: Yan, Xu
Other Authors: Zhou, Shuo , Wang, Yuanqiang , Ge, Zemei , Cheng, Tieming , Li, Runtao
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: ISSN: 0040-4020 ; E-ISSN: 1464-5416 ; DOI: 10.1016/j.tet.2012.07.004
Link: https://www.sciencedirect.com/science/article/pii/S0040402012010605
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recordid: elsevier_sdoi_10_1016_j_tet_2012_07_004
title: Propylene oxide assisted one-pot, tandem synthesis of substituted-1,3,4-oxadiazole-2(3H)-ones in water
format: Article
creator:
  • Yan, Xu
  • Zhou, Shuo
  • Wang, Yuanqiang
  • Ge, Zemei
  • Cheng, Tieming
  • Li, Runtao
subjects:
  • Substituted-1,3,4-Oxadiazole-2(3h)-Ones
  • One-Pot
  • Tandem Procedure
  • Propylene Oxide
  • Environmentally Friendly
  • Chemistry
ispartof: Tetrahedron, 23 September 2012, Vol.68(38), pp.7978-7983
description: It has been developed for the synthesis of substituted-1,3,4-oxadiazole-2(3 )-one derivatives via a novel one-pot, tandem procedure assisted by propylene oxide. The 5-substitued-1,3,4-oxadiazole-2(3 )-ones and 3,5-disubstitued-1,3,4-oxadiazole-2(3 )-ones were, respectively, obtained from three-component reaction of acylhydrazines, carbon disulfide, and propylene oxide, and four-component reaction of acylhydarazines, carbon disulfide, propylene oxide, and organic halides. The reactions were carried out using water as solvent in the presence of potassium phosphate to afford the expected products in good to excellent yields.
language: eng
source:
identifier: ISSN: 0040-4020 ; E-ISSN: 1464-5416 ; DOI: 10.1016/j.tet.2012.07.004
fulltext: fulltext
issn:
  • 0040-4020
  • 00404020
  • 1464-5416
  • 14645416
url: Link


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titlePropylene oxide assisted one-pot, tandem synthesis of substituted-1,3,4-oxadiazole-2(3H)-ones in water
creatorYan, Xu ; Zhou, Shuo ; Wang, Yuanqiang ; Ge, Zemei ; Cheng, Tieming ; Li, Runtao
ispartofTetrahedron, 23 September 2012, Vol.68(38), pp.7978-7983
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subjectSubstituted-1,3,4-Oxadiazole-2(3h)-Ones ; One-Pot ; Tandem Procedure ; Propylene Oxide ; Environmentally Friendly ; Chemistry
descriptionIt has been developed for the synthesis of substituted-1,3,4-oxadiazole-2(3 )-one derivatives via a novel one-pot, tandem procedure assisted by propylene oxide. The 5-substitued-1,3,4-oxadiazole-2(3 )-ones and 3,5-disubstitued-1,3,4-oxadiazole-2(3 )-ones were, respectively, obtained from three-component reaction of acylhydrazines, carbon disulfide, and propylene oxide, and four-component reaction of acylhydarazines, carbon disulfide, propylene oxide, and organic halides. The reactions were carried out using water as solvent in the presence of potassium phosphate to afford the expected products in good to excellent yields.
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