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Catalyst free, regioselective one-pot three-component synthesis of thiazol-2-imine derivatives in ionic liquid

A one-pot three-component approach for the synthesis of thiazol-2-imines has been described by the reaction of amine, phenyl isothiocyanate and β-nitroacrylate in [Hbim]BF4 ionic liquid. The method is applicable for aromatic, benzylic, aliphatic and cyclic amines. Reusable reaction media, regioselec... Full description

Journal Title: Tetrahedron Letters 06 November 2013, Vol.54(45), pp.5974-5978
Main Author: Santosh Kumar, G
Other Authors: Pushpa Ragini, S , Meshram, H.M
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: ISSN: 0040-4039 ; E-ISSN: 1873-3581 ; DOI: 10.1016/j.tetlet.2013.08.056
Link: http://dx.doi.org/10.1016/j.tetlet.2013.08.056
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recordid: elsevier_sdoi_10_1016_j_tetlet_2013_08_056
title: Catalyst free, regioselective one-pot three-component synthesis of thiazol-2-imine derivatives in ionic liquid
format: Article
creator:
  • Santosh Kumar, G
  • Pushpa Ragini, S
  • Meshram, H.M
subjects:
  • Amine
  • Phenyl Isothiocyanate
  • Β-Nitroacrylate
  • Thiazol-2-Imines
  • Regioselectivity and Ionic Liquid
  • Amine
  • Phenyl Isothiocyanate
  • Β-Nitroacrylate
  • Thiazol-2-Imines
  • Regioselectivity and Ionic Liquid
  • Chemistry
ispartof: Tetrahedron Letters, 06 November 2013, Vol.54(45), pp.5974-5978
description: A one-pot three-component approach for the synthesis of thiazol-2-imines has been described by the reaction of amine, phenyl isothiocyanate and β-nitroacrylate in [Hbim]BF4 ionic liquid. The method is applicable for aromatic, benzylic, aliphatic and cyclic amines. Reusable reaction media, regioselectivity, mild reaction condition, catalyst free and high yield of products are the salient features of this protocol.
language: eng
source:
identifier: ISSN: 0040-4039 ; E-ISSN: 1873-3581 ; DOI: 10.1016/j.tetlet.2013.08.056
fulltext: fulltext
issn:
  • 0040-4039
  • 00404039
  • 1873-3581
  • 18733581
url: Link


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ispartofTetrahedron Letters, 06 November 2013, Vol.54(45), pp.5974-5978
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subjectAmine ; Phenyl Isothiocyanate ; Β-Nitroacrylate ; Thiazol-2-Imines ; Regioselectivity and Ionic Liquid ; Amine ; Phenyl Isothiocyanate ; Β-Nitroacrylate ; Thiazol-2-Imines ; Regioselectivity and Ionic Liquid ; Chemistry
descriptionA one-pot three-component approach for the synthesis of thiazol-2-imines has been described by the reaction of amine, phenyl isothiocyanate and β-nitroacrylate in [Hbim]BF4 ionic liquid. The method is applicable for aromatic, benzylic, aliphatic and cyclic amines. Reusable reaction media, regioselectivity, mild reaction condition, catalyst free and high yield of products are the salient features of this protocol.
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A one-pot three-component approach for the synthesis of thiazol-2-imines has been described by the reaction of amine, phenyl isothiocyanate and β-nitroacrylate in [Hbim]BF4 ionic liquid. The method is applicable for aromatic, benzylic, aliphatic and cyclic amines. Reusable reaction media, regioselectivity, mild reaction condition, catalyst free and high yield of products are the salient features of this protocol.

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abstract

A one-pot three-component approach for the synthesis of thiazol-2-imines has been described by the reaction of amine, phenyl isothiocyanate and β-nitroacrylate in [Hbim]BF4 ionic liquid. The method is applicable for aromatic, benzylic, aliphatic and cyclic amines. Reusable reaction media, regioselectivity, mild reaction condition, catalyst free and high yield of products are the salient features of this protocol.

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lad01Tetrahedron Letters
date2013-11-06