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Manganese-catalyzed oxidative benzylic C-H fluorination by fluoride ions.

An efficient protocol for the selective fluorination of benzylic C--H bonds is described. The process is catalyzed by manganese salen complexes and uses nucleophilic fluorine sources, such as triethylamine trihydrofluoride and KF. Reaction rates are sufficiently high (30min) to allow adoption for th... Full description

Journal Title: Angewandte Chemie (International ed. in English) June 3, 2013, Vol.52(23), pp.6024-6027
Main Author: Liu, Wei
Other Authors: Groves, John T
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: E-ISSN: 1521-3773 ; DOI: 1521-3773 ; DOI: 10.1002/anie.201301097
Link: http://search.proquest.com/docview/1357493228/?pq-origsite=primo
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recordid: proquest1357493228
title: Manganese-catalyzed oxidative benzylic C-H fluorination by fluoride ions.
format: Article
creator:
  • Liu, Wei
  • Groves, John T
subjects:
  • Catalysis–Chemistry
  • Fluorides–Chemistry
  • Halogenation–Chemistry
  • Manganese–Chemistry
  • Oxidation-Reduction–Chemistry
  • Positron-Emission Tomography–Chemistry
  • Manganese
  • Fluorides
ispartof: Angewandte Chemie (International ed. in English), June 3, 2013, Vol.52(23), pp.6024-6027
description: An efficient protocol for the selective fluorination of benzylic C--H bonds is described. The process is catalyzed by manganese salen complexes and uses nucleophilic fluorine sources, such as triethylamine trihydrofluoride and KF. Reaction rates are sufficiently high (30min) to allow adoption for the incorporation of super(18)F fluoride sources for PET imaging applications.
language: eng
source:
identifier: E-ISSN: 1521-3773 ; DOI: 1521-3773 ; DOI: 10.1002/anie.201301097
fulltext: fulltext
issn:
  • 15213773
  • 1521-3773
url: Link


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descriptionAn efficient protocol for the selective fluorination of benzylic C--H bonds is described. The process is catalyzed by manganese salen complexes and uses nucleophilic fluorine sources, such as triethylamine trihydrofluoride and KF. Reaction rates are sufficiently high (30min) to allow adoption for the incorporation of super(18)F fluoride sources for PET imaging applications.
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