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ZrB2-SiC NANO-POWDER MIXTURE PREPARED USING ZrSi2 AND MODIFIED SPARK PLASMA SINTERING

ZrB2-SiC nano-powder mixture was synthesised using ZrSi2 source material and a modified spark plasma sintering apparatus. The particle size of ZrB2 and SiC was about 80 and 20 nm, respectively. The molecular-level homogeneity of Zr/Si source and fast heating/cooling rate by SPS caused the formation... Full description

Journal Title: Journal of the American Ceramic Society 2013, Vol.96(4), pp.1051-1054
Main Author: Lee, S-H
Other Authors: Choi, S-Y , Kim, H-D
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: ISSN: 0002-7820
Link: http://search.proquest.com/docview/1417929935/?pq-origsite=primo
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title: ZrB2-SiC NANO-POWDER MIXTURE PREPARED USING ZrSi2 AND MODIFIED SPARK PLASMA SINTERING
format: Article
creator:
  • Lee, S-H
  • Choi, S-Y
  • Kim, H-D
subjects:
  • Homogeneity
  • Ceramics
  • Nanomaterials
  • Inert
  • Nanocomposites
  • Silicon Carbide
  • Nanostructure
  • Spark Plasma Sintering
  • General (Wc)
  • General and Nonclassified (EC)
ispartof: Journal of the American Ceramic Society, 2013, Vol.96(4), pp.1051-1054
description: ZrB2-SiC nano-powder mixture was synthesised using ZrSi2 source material and a modified spark plasma sintering apparatus. The particle size of ZrB2 and SiC was about 80 and 20 nm, respectively. The molecular-level homogeneity of Zr/Si source and fast heating/cooling rate by SPS caused the formation of homogeneously intermixed nano-powders. A strong exothermal reaction occurred at around 860 C, causing strong agglomeration and growth of the synthesised powder mixture. The rapid reaction could be controlled by adding 20 wt% of NaCl, which acted as an inert filler.
language: eng
source:
identifier: ISSN: 0002-7820
fulltext: fulltext
issn:
  • 00027820
  • 0002-7820
url: Link


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titleZrB2-SiC NANO-POWDER MIXTURE PREPARED USING ZrSi2 AND MODIFIED SPARK PLASMA SINTERING
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subjectHomogeneity ; Ceramics ; Nanomaterials ; Inert ; Nanocomposites ; Silicon Carbide ; Nanostructure ; Spark Plasma Sintering ; General (Wc) ; General and Nonclassified (EC)
descriptionZrB2-SiC nano-powder mixture was synthesised using ZrSi2 source material and a modified spark plasma sintering apparatus. The particle size of ZrB2 and SiC was about 80 and 20 nm, respectively. The molecular-level homogeneity of Zr/Si source and fast heating/cooling rate by SPS caused the formation of homogeneously intermixed nano-powders. A strong exothermal reaction occurred at around 860 C, causing strong agglomeration and growth of the synthesised powder mixture. The rapid reaction could be controlled by adding 20 wt% of NaCl, which acted as an inert filler.
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descriptionZrB2-SiC nano-powder mixture was synthesised using ZrSi2 source material and a modified spark plasma sintering apparatus. The particle size of ZrB2 and SiC was about 80 and 20 nm, respectively. The molecular-level homogeneity of Zr/Si source and fast heating/cooling rate by SPS caused the formation of homogeneously intermixed nano-powders. A strong exothermal reaction occurred at around 860 C, causing strong agglomeration and growth of the synthesised powder mixture. The rapid reaction could be controlled by adding 20 wt% of NaCl, which acted as an inert filler.
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abstractZrB2-SiC nano-powder mixture was synthesised using ZrSi2 source material and a modified spark plasma sintering apparatus. The particle size of ZrB2 and SiC was about 80 and 20 nm, respectively. The molecular-level homogeneity of Zr/Si source and fast heating/cooling rate by SPS caused the formation of homogeneously intermixed nano-powders. A strong exothermal reaction occurred at around 860 C, causing strong agglomeration and growth of the synthesised powder mixture. The rapid reaction could be controlled by adding 20 wt% of NaCl, which acted as an inert filler.
urlhttp://search.proquest.com/docview/1417929935/
doi10.1111/jace.12267
eissn15512916
date2013-04