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Development and Validation of Spectrophotometric Methods for Estimating Amisulpride in Pharmaceutical Preparations

  Five simple, sensitive, accurate and rapid visible spectrophotometric methods (A, B, C, D and E) have been developed for estimating Amisulpride in pharmaceutical preparations. These are based on the diazotization of Amisulpride with sodium nitrite and hydrochloric acid, followed by coupling with N... Full description

Journal Title: Analytical Sciences 2010, Vol.26(4), p.485
Main Author: Sharma, Sangita
Other Authors: Neog, Madhurjya , Prajapati, Vipul , Patel, Hiren , Dabhi, Dipti
Format: Electronic Article Electronic Article
Language: English
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ID: ISSN: 09106340 ; E-ISSN: 13482246
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title: Development and Validation of Spectrophotometric Methods for Estimating Amisulpride in Pharmaceutical Preparations
format: Article
creator:
  • Sharma, Sangita
  • Neog, Madhurjya
  • Prajapati, Vipul
  • Patel, Hiren
  • Dabhi, Dipti
subjects:
  • Chemistry
ispartof: Analytical Sciences, 2010, Vol.26(4), p.485
description:   Five simple, sensitive, accurate and rapid visible spectrophotometric methods (A, B, C, D and E) have been developed for estimating Amisulpride in pharmaceutical preparations. These are based on the diazotization of Amisulpride with sodium nitrite and hydrochloric acid, followed by coupling with N-(1-naphthyl)ethylenediamine dihydrochloride (Method A), diphenylamine (Method B), β-naphthol in an alkaline medium (Method C), resorcinol in an alkaline medium (Method D) and chromotropic acid in an alkaline medium (Method E) to form a colored chromogen. The absorption maxima, λmax, are at 523 nm for Method A, 382 and 490 nm for Method B, 527 nm for Method C, 521 nm for Method D and 486 nm for Method E. Beer's law was obeyed in the concentration range of 2.5 - 12.5 μg mL-1 in Method A, 5 - 25 and 10 - 50 μg mL-1 in Method B, 4 - 20 μg mL-1 in Method C, 2.5 - 12.5 μg mL-1 in Method D and 5 - 15 μg mL-1...
language: eng
source:
identifier: ISSN: 09106340 ; E-ISSN: 13482246
fulltext: fulltext
issn:
  • 09106340
  • 0910-6340
  • 13482246
  • 1348-2246
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titleDevelopment and Validation of Spectrophotometric Methods for Estimating Amisulpride in Pharmaceutical Preparations
creatorSharma, Sangita ; Neog, Madhurjya ; Prajapati, Vipul ; Patel, Hiren ; Dabhi, Dipti
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identifierISSN: 09106340 ; E-ISSN: 13482246
description  Five simple, sensitive, accurate and rapid visible spectrophotometric methods (A, B, C, D and E) have been developed for estimating Amisulpride in pharmaceutical preparations. These are based on the diazotization of Amisulpride with sodium nitrite and hydrochloric acid, followed by coupling with N-(1-naphthyl)ethylenediamine dihydrochloride (Method A), diphenylamine (Method B), β-naphthol in an alkaline medium (Method C), resorcinol in an alkaline medium (Method D) and chromotropic acid in an alkaline medium (Method E) to form a colored chromogen. The absorption maxima, λmax, are at 523 nm for Method A, 382 and 490 nm for Method B, 527 nm for Method C, 521 nm for Method D and 486 nm for Method E. Beer's law was obeyed in the concentration range of 2.5 - 12.5 μg mL-1 in Method A, 5 - 25 and 10 - 50 μg mL-1 in Method B, 4 - 20 μg mL-1 in Method C, 2.5 - 12.5 μg mL-1 in Method D and 5 - 15 μg mL-1...
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description  Five simple, sensitive, accurate and rapid visible spectrophotometric methods (A, B, C, D and E) have been developed for estimating Amisulpride in pharmaceutical preparations. These are based on the diazotization of Amisulpride with sodium nitrite and hydrochloric acid, followed by coupling with N-(1-naphthyl)ethylenediamine dihydrochloride (Method A), diphenylamine (Method B), β-naphthol in an alkaline medium (Method C), resorcinol in an alkaline medium (Method D) and chromotropic acid in an alkaline medium (Method E) to form a colored chromogen. The absorption maxima, λmax, are at 523 nm for Method A, 382 and 490 nm for Method B, 527 nm for Method C, 521 nm for Method D and 486 nm for Method E. Beer's law was obeyed in the concentration range of 2.5 - 12.5 μg mL-1 in Method A, 5 - 25 and 10 - 50 μg mL-1 in Method B, 4 - 20 μg mL-1 in Method C, 2.5 - 12.5 μg mL-1 in Method D and 5 - 15 μg mL-1...
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abstract  Five simple, sensitive, accurate and rapid visible spectrophotometric methods (A, B, C, D and E) have been developed for estimating Amisulpride in pharmaceutical preparations. These are based on the diazotization of Amisulpride with sodium nitrite and hydrochloric acid, followed by coupling with N-(1-naphthyl)ethylenediamine dihydrochloride (Method A), diphenylamine (Method B), β-naphthol in an alkaline medium (Method C), resorcinol in an alkaline medium (Method D) and chromotropic acid in an alkaline medium (Method E) to form a colored chromogen. The absorption maxima, λmax, are at 523 nm for Method A, 382 and 490 nm for Method B, 527 nm for Method C, 521 nm for Method D and 486 nm for Method E. Beer's law was obeyed in the concentration range of 2.5 - 12.5 μg mL-1 in Method A, 5 - 25 and 10 - 50 μg mL-1 in Method B, 4 - 20 μg mL-1 in Method C, 2.5 - 12.5 μg mL-1 in Method D and 5 - 15 μg mL-1...
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