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Design and synthesis of organosoluble and transparent polyimides containing bulky substituents and noncoplanar structures

  A new diamine monomer, 3,3'-diisopropyl-4,4'-diaminophenyl-4''-phenyltouene, was designed, synthesized, and then polymerized with five commercial dianhydrides to obtain a series of novel polyimides via a one-step method. The obtained polymers showed excellent solubility in most common solvents, ev... Full description

Journal Title: Journal of Applied Polymer Science Apr 10, 2016, Vol.133(14)
Main Author: Huang, Xiaohua
Other Authors: Pei, Xianglin , Wang, Lichun , Mei, Mei , Liu, Chanjuan , Wei, Chun
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: ISSN: 00218995 ; E-ISSN: 10974628 ; DOI: 10.1002/app.43266
Link: http://search.proquest.com/docview/1755262730/?pq-origsite=primo
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title: Design and synthesis of organosoluble and transparent polyimides containing bulky substituents and noncoplanar structures
format: Article
creator:
  • Huang, Xiaohua
  • Pei, Xianglin
  • Wang, Lichun
  • Mei, Mei
  • Liu, Chanjuan
  • Wei, Chun
subjects:
  • Polyimides – Optical Properties
ispartof: Journal of Applied Polymer Science, Apr 10, 2016, Vol.133(14)
description:   A new diamine monomer, 3,3'-diisopropyl-4,4'-diaminophenyl-4''-phenyltouene, was designed, synthesized, and then polymerized with five commercial dianhydrides to obtain a series of novel polyimides via a one-step method. The obtained polymers showed excellent solubility in most common solvents, even in low-boiling solvents, such as chloroform, dichloromethane, and tetrahydrofuran. They exhibited a high thermal stability with the glass-transition temperature in the range 262-318°C and 10% weight loss temperatures in the range 464-488°C under a nitrogen atmospheres. Meanwhile, these polymer films also displayed a high optical transparency with a cutoff wavelength in the range 305-365 nm; prominent mechanical properties with a tensile strength of 65.6-94.9 MPa, a Young's modulus of 1.6-2.8 GPa, and an elongation at break of 9.3-13.7%; a low dielectric constant in the range of 2.91-3.18 at 1 MHz;...
language: eng
source:
identifier: ISSN: 00218995 ; E-ISSN: 10974628 ; DOI: 10.1002/app.43266
fulltext: fulltext
issn:
  • 00218995
  • 0021-8995
  • 10974628
  • 1097-4628
url: Link


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titleDesign and synthesis of organosoluble and transparent polyimides containing bulky substituents and noncoplanar structures
creatorHuang, Xiaohua ; Pei, Xianglin ; Wang, Lichun ; Mei, Mei ; Liu, Chanjuan ; Wei, Chun
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description  A new diamine monomer, 3,3'-diisopropyl-4,4'-diaminophenyl-4''-phenyltouene, was designed, synthesized, and then polymerized with five commercial dianhydrides to obtain a series of novel polyimides via a one-step method. The obtained polymers showed excellent solubility in most common solvents, even in low-boiling solvents, such as chloroform, dichloromethane, and tetrahydrofuran. They exhibited a high thermal stability with the glass-transition temperature in the range 262-318°C and 10% weight loss temperatures in the range 464-488°C under a nitrogen atmospheres. Meanwhile, these polymer films also displayed a high optical transparency with a cutoff wavelength in the range 305-365 nm; prominent mechanical properties with a tensile strength of 65.6-94.9 MPa, a Young's modulus of 1.6-2.8 GPa, and an elongation at break of 9.3-13.7%; a low dielectric constant in the range of 2.91-3.18 at 1 MHz;...
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titleDesign and synthesis of organosoluble and transparent polyimides containing bulky substituents and noncoplanar structures
description  A new diamine monomer, 3,3'-diisopropyl-4,4'-diaminophenyl-4''-phenyltouene, was designed, synthesized, and then polymerized with five commercial dianhydrides to obtain a series of novel polyimides via a one-step method. The obtained polymers showed excellent solubility in most common solvents, even in low-boiling solvents, such as chloroform, dichloromethane, and tetrahydrofuran. They exhibited a high thermal stability with the glass-transition temperature in the range 262-318°C and 10% weight loss temperatures in the range 464-488°C under a nitrogen atmospheres. Meanwhile, these polymer films also displayed a high optical transparency with a cutoff wavelength in the range 305-365 nm; prominent mechanical properties with a tensile strength of 65.6-94.9 MPa, a Young's modulus of 1.6-2.8 GPa, and an elongation at break of 9.3-13.7%; a low dielectric constant in the range of 2.91-3.18 at 1 MHz;...
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abstract  A new diamine monomer, 3,3'-diisopropyl-4,4'-diaminophenyl-4''-phenyltouene, was designed, synthesized, and then polymerized with five commercial dianhydrides to obtain a series of novel polyimides via a one-step method. The obtained polymers showed excellent solubility in most common solvents, even in low-boiling solvents, such as chloroform, dichloromethane, and tetrahydrofuran. They exhibited a high thermal stability with the glass-transition temperature in the range 262-318°C and 10% weight loss temperatures in the range 464-488°C under a nitrogen atmospheres. Meanwhile, these polymer films also displayed a high optical transparency with a cutoff wavelength in the range 305-365 nm; prominent mechanical properties with a tensile strength of 65.6-94.9 MPa, a Young's modulus of 1.6-2.8 GPa, and an elongation at break of 9.3-13.7%; a low dielectric constant in the range of 2.91-3.18 at 1 MHz;...
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