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Concise Enantiospecific Total Synthesis of Tubingensin A

We report the enantiospecific total synthesis of (+)-tubingensin A. Our synthesis features an aryne cyclization to efficiently introduce the vicinal quaternary stereocenters of the natural product and proceeds in only nine steps (longest linear sequence) from known compounds.

Journal Title: Journal of the American Chemical Society 20140214, Vol.136(8), pp.3036-3039
Main Author: Goetz, Adam
Other Authors: Silberstein, Amanda , Corsello, Michael , Garg, Neil
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: ISSN: 0002-7863 ; E-ISSN: 1520-5126 ; DOI: 10.1021/ja501142e
Link: http://search.proquest.com/docview/1762073189/?pq-origsite=primo
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recordid: proquest1762073189
title: Concise Enantiospecific Total Synthesis of Tubingensin A
format: Article
creator:
  • Goetz, Adam
  • Silberstein, Amanda
  • Corsello, Michael
  • Garg, Neil
subjects:
  • Natural Products
  • Synthesis
  • Analysis (MD)
  • Chemical Analysis (Ep)
  • Chemical Analysis (Ed)
  • Chemical Analysis (EC)
ispartof: Journal of the American Chemical Society, 20140214, Vol.136(8), pp.3036-3039
description: We report the enantiospecific total synthesis of (+)-tubingensin A. Our synthesis features an aryne cyclization to efficiently introduce the vicinal quaternary stereocenters of the natural product and proceeds in only nine steps (longest linear sequence) from known compounds.
language: eng
source:
identifier: ISSN: 0002-7863 ; E-ISSN: 1520-5126 ; DOI: 10.1021/ja501142e
fulltext: no_fulltext
issn:
  • 00027863
  • 0002-7863
  • 15205126
  • 1520-5126
url: Link


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descriptionWe report the enantiospecific total synthesis of (+)-tubingensin A. Our synthesis features an aryne cyclization to efficiently introduce the vicinal quaternary stereocenters of the natural product and proceeds in only nine steps (longest linear sequence) from known compounds.
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abstractWe report the enantiospecific total synthesis of (+)-tubingensin A. Our synthesis features an aryne cyclization to efficiently introduce the vicinal quaternary stereocenters of the natural product and proceeds in only nine steps (longest linear sequence) from known compounds.
doi10.1021/ja501142e
urlhttp://search.proquest.com/docview/1762073189/
date2014-02-26