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Synthesis hexagonal ß-Ni(OH) 2 nanosheets for use in electrochemistry sensors

Hexagonal β-Ni(OH) 2 nanosheets were synthesized by a simple template- and surfactant-free hydrothermal approach. They were characterized by scanning electron microscopy, X-ray powder diffraction, and thermal gravimetric analysis. The nanosheets were incorporated, along with chitosan, into an ampero... Full description

Journal Title: Microchimica Acta 2009, Vol.167(1), pp.47-52
Main Author: Fang, Bin
Other Authors: Gu, Aixia , Wang, Guangfeng , Li, Bo , Zhang, Cuihong , Fang, Yongyi , Zhang, Xiaojun
Format: Electronic Article Electronic Article
Language: English
Subjects:
HO
ID: ISSN: 0026-3672 ; E-ISSN: 1436-5073 ; DOI: 10.1007/s00604-009-0213-8
Link: http://dx.doi.org/10.1007/s00604-009-0213-8
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recordid: springer_jour10.1007/s00604-009-0213-8
title: Synthesis hexagonal ß-Ni(OH) 2 nanosheets for use in electrochemistry sensors
format: Article
creator:
  • Fang, Bin
  • Gu, Aixia
  • Wang, Guangfeng
  • Li, Bo
  • Zhang, Cuihong
  • Fang, Yongyi
  • Zhang, Xiaojun
subjects:
  • β-Ni(OH)
  • Electrochemistry sensor
  • Pyrocatechol
  • Hydroquinone
  • HO
ispartof: Microchimica Acta, 2009, Vol.167(1), pp.47-52
description: Hexagonal β-Ni(OH) 2 nanosheets were synthesized by a simple template- and surfactant-free hydrothermal approach. They were characterized by scanning electron microscopy, X-ray powder diffraction, and thermal gravimetric analysis. The nanosheets were incorporated, along with chitosan, into an amperometric sensor which displayed a good performance in terms of detection of hydrogen peroxide. The linear range is from 5.0 µM to 0.145 mM, the sensitivity is 24.76 µA mM −1 , the detection limit is 0.5 µM, and the response time is
language: eng
source:
identifier: ISSN: 0026-3672 ; E-ISSN: 1436-5073 ; DOI: 10.1007/s00604-009-0213-8
fulltext: fulltext
issn:
  • 1436-5073
  • 14365073
  • 0026-3672
  • 00263672
url: Link


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titleSynthesis hexagonal ß-Ni(OH) 2 nanosheets for use in electrochemistry sensors
creatorFang, Bin ; Gu, Aixia ; Wang, Guangfeng ; Li, Bo ; Zhang, Cuihong ; Fang, Yongyi ; Zhang, Xiaojun
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descriptionHexagonal β-Ni(OH) 2 nanosheets were synthesized by a simple template- and surfactant-free hydrothermal approach. They were characterized by scanning electron microscopy, X-ray powder diffraction, and thermal gravimetric analysis. The nanosheets were incorporated, along with chitosan, into an amperometric sensor which displayed a good performance in terms of detection of hydrogen peroxide. The linear range is from 5.0 µM to 0.145 mM, the sensitivity is 24.76 µA mM −1 , the detection limit is 0.5 µM, and the response time is <5 s. The sensor was successfully applied to detect pyrocatechol (PC) and hydroquinone (HQ) via cyclic voltammetry and differential pulse voltammetry and also enabled simultaneous determination of both PC and HQ.
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descriptionHexagonal β-Ni(OH) 2 nanosheets were synthesized by a simple template- and surfactant-free hydrothermal approach. They were characterized by scanning electron microscopy, X-ray powder diffraction, and thermal gravimetric analysis. The nanosheets were incorporated, along with chitosan, into an amperometric sensor which displayed a good performance in terms of detection of hydrogen peroxide. The linear range is from 5.0 µM to 0.145 mM, the sensitivity is 24.76 µA mM −1 , the detection limit is 0.5 µM, and the response time is <5 s. The sensor was successfully applied to detect pyrocatechol (PC) and hydroquinone (HQ) via cyclic voltammetry and differential pulse voltammetry and also enabled simultaneous determination of both PC and HQ.
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abstractHexagonal β-Ni(OH) 2 nanosheets were synthesized by a simple template- and surfactant-free hydrothermal approach. They were characterized by scanning electron microscopy, X-ray powder diffraction, and thermal gravimetric analysis. The nanosheets were incorporated, along with chitosan, into an amperometric sensor which displayed a good performance in terms of detection of hydrogen peroxide. The linear range is from 5.0 µM to 0.145 mM, the sensitivity is 24.76 µA mM −1 , the detection limit is 0.5 µM, and the response time is <5 s. The sensor was successfully applied to detect pyrocatechol (PC) and hydroquinone (HQ) via cyclic voltammetry and differential pulse voltammetry and also enabled simultaneous determination of both PC and HQ.
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