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Three New Complexes Based on a Flexible Bis(benzimidazole) Ligand and Rigid/Flexible Organic Carboxylates

Byline: Xiu-Li Wang (1), Jin-Xia Zhang (1), Li-Li Hou (1), Ju-Wen Zhang (1), Guo-Cheng Liu (1), Hong-Yan Lin (1) Keywords: Hydrothermal synthesis; Crystal structures; Benzimidazole; Organic carboxylate; Luminescent property Abstract: Abstract Three new polymeric frameworks, [Ni(bbbm)(L1).sub.2].sub.... Full description

Journal Title: Journal of Chemical Crystallography 2011, Vol.41(10), pp.1579-1585
Main Author: Wang, Xiu-Li
Other Authors: Zhang, Jin-Xia , Hou, Li-Li , Zhang, Ju-Wen , Liu, Guo-Cheng , Lin, Hong-Yan
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: ISSN: 1074-1542 ; E-ISSN: 1572-8854 ; DOI: 10.1007/s10870-011-0143-2
Link: http://dx.doi.org/10.1007/s10870-011-0143-2
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recordid: springer_jour10.1007/s10870-011-0143-2
title: Three New Complexes Based on a Flexible Bis(benzimidazole) Ligand and Rigid/Flexible Organic Carboxylates
format: Article
creator:
  • Wang, Xiu-Li
  • Zhang, Jin-Xia
  • Hou, Li-Li
  • Zhang, Ju-Wen
  • Liu, Guo-Cheng
  • Lin, Hong-Yan
subjects:
  • Hydrothermal synthesis
  • Crystal structures
  • Benzimidazole
  • Organic carboxylate
  • Luminescent property
ispartof: Journal of Chemical Crystallography, 2011, Vol.41(10), pp.1579-1585
description: Byline: Xiu-Li Wang (1), Jin-Xia Zhang (1), Li-Li Hou (1), Ju-Wen Zhang (1), Guo-Cheng Liu (1), Hong-Yan Lin (1) Keywords: Hydrothermal synthesis; Crystal structures; Benzimidazole; Organic carboxylate; Luminescent property Abstract: Abstract Three new polymeric frameworks, [Ni(bbbm)(L1).sub.2].sub.n (1), [Ni(bbbm)(L2).sub.2].sub.n (2), and {[Co(bbbm)(L3)]*[H.sub.2]O}.sub.n (3) (bbbm = 1,4-bis(N-benzimidazolyl) butane, HL1 = 4-bromobenzoic acid, HL2 = 3-methylbenzoic acid, and [H.sub.2]L3 = glutaric acid) have been hydrothermally synthesized and structurally characterized by single-crystal X-ray diffraction. Complex 1 features a one-dimensional (1D) linear chain structure bridged by bbbm ligands, which is further connected into a supramolecular double chain structure through intermolecular [pi]--[pi] stacking interactions. Complex 2 contains 1D zigzag chain, which is further arranged into a 2D supramolecular architecture by hydrogen bonding and [pi]--[pi] stacking interactions. In the structure of 3, there are infinite 1D zigzag Co(II)-bbbm chains linked together by L3 ligands to generate an undulated 2D (4,4) sheet, which is further connected by intermolecular [pi]--[pi] stacking interactions to form a 3D supramolecular network. Furthermore, thermal stability and luminescent property of 1--3 were investigated. Graphical Abstract Three new two/three-dimensional supramolecular complexes [Ni(bbbm)(L1).sub.2].sub.n (1), [Ni(bbbm)(L2).sub.2].sub.n (2), and {[Co(bbbm)(L3)]*[H.sub.2]O}.sub.n (3) [bbbm = 1,4-bis(N-benzimidazolyl) butane] have been synthesized from hydrothermal reaction of a metal salt with ligands: bbbm and one carboxylate ligand, 4-bromobenzoic acid (HL1), 3-methylbenzoic (HL2), and glutaric acid ([H.sub.2]L3). Author Affiliation: (1) Department of Chemistry, Bohai University, Jinzhou, 121000, People's Republic of China Article History: Registration Date: 28/05/2011 Received Date: 09/04/2011 Accepted Date: 28/05/2011 Online Date: 10/06/2011
language: eng
source:
identifier: ISSN: 1074-1542 ; E-ISSN: 1572-8854 ; DOI: 10.1007/s10870-011-0143-2
fulltext: fulltext
issn:
  • 1572-8854
  • 15728854
  • 1074-1542
  • 10741542
url: Link


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titleThree New Complexes Based on a Flexible Bis(benzimidazole) Ligand and Rigid/Flexible Organic Carboxylates
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descriptionByline: Xiu-Li Wang (1), Jin-Xia Zhang (1), Li-Li Hou (1), Ju-Wen Zhang (1), Guo-Cheng Liu (1), Hong-Yan Lin (1) Keywords: Hydrothermal synthesis; Crystal structures; Benzimidazole; Organic carboxylate; Luminescent property Abstract: Abstract Three new polymeric frameworks, [Ni(bbbm)(L1).sub.2].sub.n (1), [Ni(bbbm)(L2).sub.2].sub.n (2), and {[Co(bbbm)(L3)]*[H.sub.2]O}.sub.n (3) (bbbm = 1,4-bis(N-benzimidazolyl) butane, HL1 = 4-bromobenzoic acid, HL2 = 3-methylbenzoic acid, and [H.sub.2]L3 = glutaric acid) have been hydrothermally synthesized and structurally characterized by single-crystal X-ray diffraction. Complex 1 features a one-dimensional (1D) linear chain structure bridged by bbbm ligands, which is further connected into a supramolecular double chain structure through intermolecular [pi]--[pi] stacking interactions. Complex 2 contains 1D zigzag chain, which is further arranged into a 2D supramolecular architecture by hydrogen bonding and [pi]--[pi] stacking interactions. In the structure of 3, there are infinite 1D zigzag Co(II)-bbbm chains linked together by L3 ligands to generate an undulated 2D (4,4) sheet, which is further connected by intermolecular [pi]--[pi] stacking interactions to form a 3D supramolecular network. Furthermore, thermal stability and luminescent property of 1--3 were investigated. Graphical Abstract Three new two/three-dimensional supramolecular complexes [Ni(bbbm)(L1).sub.2].sub.n (1), [Ni(bbbm)(L2).sub.2].sub.n (2), and {[Co(bbbm)(L3)]*[H.sub.2]O}.sub.n (3) [bbbm = 1,4-bis(N-benzimidazolyl) butane] have been synthesized from hydrothermal reaction of a metal salt with ligands: bbbm and one carboxylate ligand, 4-bromobenzoic acid (HL1), 3-methylbenzoic (HL2), and glutaric acid ([H.sub.2]L3). Author Affiliation: (1) Department of Chemistry, Bohai University, Jinzhou, 121000, People's Republic of China Article History: Registration Date: 28/05/2011 Received Date: 09/04/2011 Accepted Date: 28/05/2011 Online Date: 10/06/2011
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