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A highly sensitive fluorescent bulk sensor based on isonicotinic acid hydrazide–immobilized nano-fumed silica (fumed-Si–INAH) for detection of Hg 2+ and Cr 3+ ions in aqueous media

Through functionalizing of isonicotinic acid hydrazide (INAH) on to fumed silica nanoparticles, a novel fluorescent nanomaterial (fumed-Si–INAH) was synthesized and characterized using various techniques including FT-IR, SEM, and TGA. Next, interaction of the new nanofluorophore material with metal... Full description

Journal Title: Journal of the Iranian Chemical Society 2018, Vol.15(1), pp.211-221
Main Author: Mohammadi Ziarani, Ghodsi
Other Authors: Fathi Vavsari, Vaezeh , Badiei, Alireza , Afshani, Jafar , Gholamzadeh, Parisa , Balalaie, Saeed , Faridbod, Farnoush , Ganjali, Mohammad
Format: Electronic Article Electronic Article
Language: English
Subjects:
ID: ISSN: 1735-207X ; E-ISSN: 1735-2428 ; DOI: 10.1007/s13738-017-1225-7
Link: http://dx.doi.org/10.1007/s13738-017-1225-7
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recordid: springer_jour10.1007/s13738-017-1225-7
title: A highly sensitive fluorescent bulk sensor based on isonicotinic acid hydrazide–immobilized nano-fumed silica (fumed-Si–INAH) for detection of Hg 2+ and Cr 3+ ions in aqueous media
format: Article
creator:
  • Mohammadi Ziarani, Ghodsi
  • Fathi Vavsari, Vaezeh
  • Badiei, Alireza
  • Afshani, Jafar
  • Gholamzadeh, Parisa
  • Balalaie, Saeed
  • Faridbod, Farnoush
  • Ganjali, Mohammad
subjects:
  • Optical sensor
  • Nano-silica
  • Hybrid materials
  • Fluorescence
  • Isonicotinic acid hydrazide
ispartof: Journal of the Iranian Chemical Society, 2018, Vol.15(1), pp.211-221
description: Through functionalizing of isonicotinic acid hydrazide (INAH) on to fumed silica nanoparticles, a novel fluorescent nanomaterial (fumed-Si–INAH) was synthesized and characterized using various techniques including FT-IR, SEM, and TGA. Next, interaction of the new nanofluorophore material with metal cations was studied spectrofluorimetrically. The fluorescence evaluation of fumed-Si–INAH towards a wide range of cations including Pb2+, Cd2+, Zn2+, Cu2+, Fe2+, Ca2+, Ni2+, Mn2+, Mg2+, Co2+, Na+, Hg2+, Cr3+, and K+ revealed that fumed-Si–INAH was a highly selective optical sensor for Hg2+ and Cr3+ ions in a wide range of pH in water. Thus, it was applied as a fluorescent bulk sensor for Hg2+ and Cr3+ ions. The detection limits were obtained to be 3.5 × 10−5 and 4.2 × 10−5 M for Hg2+ and Cr3+, respectively. Graphical abstract
language: eng
source:
identifier: ISSN: 1735-207X ; E-ISSN: 1735-2428 ; DOI: 10.1007/s13738-017-1225-7
fulltext: fulltext
issn:
  • 1735-2428
  • 17352428
  • 1735-207X
  • 1735207X
url: Link


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titleA highly sensitive fluorescent bulk sensor based on isonicotinic acid hydrazide–immobilized nano-fumed silica (fumed-Si–INAH) for detection of Hg 2+ and Cr 3+ ions in aqueous media
creatorMohammadi Ziarani, Ghodsi ; Fathi Vavsari, Vaezeh ; Badiei, Alireza ; Afshani, Jafar ; Gholamzadeh, Parisa ; Balalaie, Saeed ; Faridbod, Farnoush ; Ganjali, Mohammad
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descriptionThrough functionalizing of isonicotinic acid hydrazide (INAH) on to fumed silica nanoparticles, a novel fluorescent nanomaterial (fumed-Si–INAH) was synthesized and characterized using various techniques including FT-IR, SEM, and TGA. Next, interaction of the new nanofluorophore material with metal cations was studied spectrofluorimetrically. The fluorescence evaluation of fumed-Si–INAH towards a wide range of cations including Pb2+, Cd2+, Zn2+, Cu2+, Fe2+, Ca2+, Ni2+, Mn2+, Mg2+, Co2+, Na+, Hg2+, Cr3+, and K+ revealed that fumed-Si–INAH was a highly selective optical sensor for Hg2+ and Cr3+ ions in a wide range of pH in water. Thus, it was applied as a fluorescent bulk sensor for Hg2+ and Cr3+ ions. The detection limits were obtained to be 3.5 × 10−5 and 4.2 × 10−5 M for Hg2+ and Cr3+, respectively. Graphical abstract
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titleA highly sensitive fluorescent bulk sensor based on isonicotinic acid hydrazide–immobilized nano-fumed silica (fumed-Si–INAH) for detection of Hg 2+ and Cr 3+ ions in aqueous media
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