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Synthesis of Pyridophenanthrolines via a Three‐Component Reaction Involving 1,10‐Phenanthrolin‐5‐Amine

A facile and efficient method for the synthesis of benzo[]pyrido[3,2‐][1,7]phenanthrolines and dipyrido[4,3‐:3′,2′‐][1,7]phenanthrolines has been developed in high yields. Using EtOH as a solvent without any additionally basic catalysts, the three‐component reaction of aromatic aldehyde, 1,10‐phenan... Full description

Journal Title: Journal of Heterocyclic Chemistry July 2017, Vol.54(4), pp.2266-2271
Main Author: Miao, Wei‐Qing
Other Authors: Zhang, Mei‐Mei , Wang, Xiang‐Shan
Format: Electronic Article Electronic Article
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ID: ISSN: 0022-152X ; E-ISSN: 1943-5193 ; DOI: 10.1002/jhet.2814
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recordid: wj10.1002/jhet.2814
title: Synthesis of Pyridophenanthrolines via a Three‐Component Reaction Involving 1,10‐Phenanthrolin‐5‐Amine
format: Article
creator:
  • Miao, Wei‐Qing
  • Zhang, Mei‐Mei
  • Wang, Xiang‐Shan
subjects:
  • Amines
  • Pyridine
ispartof: Journal of Heterocyclic Chemistry, July 2017, Vol.54(4), pp.2266-2271
description: A facile and efficient method for the synthesis of benzo[]pyrido[3,2‐][1,7]phenanthrolines and dipyrido[4,3‐:3′,2′‐][1,7]phenanthrolines has been developed in high yields. Using EtOH as a solvent without any additionally basic catalysts, the three‐component reaction of aromatic aldehyde, 1,10‐phenanthrolin‐5‐amine, and dimedone or piperidine‐2,4‐dione affords two novel classes of fused phentacyclic heterocycles containing both pyridine and phenanthroline moieties.
language:
source:
identifier: ISSN: 0022-152X ; E-ISSN: 1943-5193 ; DOI: 10.1002/jhet.2814
fulltext: fulltext
issn:
  • 0022-152X
  • 0022152X
  • 1943-5193
  • 19435193
url: Link


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titleSynthesis of Pyridophenanthrolines via a Three‐Component Reaction Involving 1,10‐Phenanthrolin‐5‐Amine
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descriptionA facile and efficient method for the synthesis of benzo[]pyrido[3,2‐][1,7]phenanthrolines and dipyrido[4,3‐:3′,2′‐][1,7]phenanthrolines has been developed in high yields. Using EtOH as a solvent without any additionally basic catalysts, the three‐component reaction of aromatic aldehyde, 1,10‐phenanthrolin‐5‐amine, and dimedone or piperidine‐2,4‐dione affords two novel classes of fused phentacyclic heterocycles containing both pyridine and phenanthroline moieties.
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titleSynthesis of Pyridophenanthrolines via a Three‐Component Reaction Involving 1,10‐Phenanthrolin‐5‐Amine
descriptionA facile and efficient method for the synthesis of benzo[]pyrido[3,2‐][1,7]phenanthrolines and dipyrido[4,3‐:3′,2′‐][1,7]phenanthrolines has been developed in high yields. Using EtOH as a solvent without any additionally basic catalysts, the three‐component reaction of aromatic aldehyde, 1,10‐phenanthrolin‐5‐amine, and dimedone or piperidine‐2,4‐dione affords two novel classes of fused phentacyclic heterocycles containing both pyridine and phenanthroline moieties.
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abstractA facile and efficient method for the synthesis of benzo[]pyrido[3,2‐][1,7]phenanthrolines and dipyrido[4,3‐:3′,2′‐][1,7]phenanthrolines has been developed in high yields. Using EtOH as a solvent without any additionally basic catalysts, the three‐component reaction of aromatic aldehyde, 1,10‐phenanthrolin‐5‐amine, and dimedone or piperidine‐2,4‐dione affords two novel classes of fused phentacyclic heterocycles containing both pyridine and phenanthroline moieties.
doi10.1002/jhet.2814
pages2266-2271
date2017-07